(단종/별도문의)SOLID PHASE EXTRACTION >

SPE(Solid-phase extraction)를 새롭게 사용하는 혹은 기존 사용자들에게 최신 SPE 사용법과 사용할 분야는 물론, SPE의 최신 설비 및 기법들을 소개하고 있다. 파트 I은 SPE 발전 기술, 문제 해결 및 최적화 방법은 물론 SPE 이론, 화학, 메카니즘을 포함하는 기본적인 SPE 컨셉을 설명하고 있다. 파트 II에서는 실제 생활에서부터 도출되는 예들을 통하여 의학, 환경, 자연 제품 화학에서의 SPE 응용을 고찰하고 있다. 파트 III에서는 자동 공정, SPE disk, microextraction과 같은 혁신적인 것들에 관한 웹사이트 리스트와 제품 가이드를 포함하여 최신 SPE 기술을 논의한다.


SPE 사용 범위를 기술하는 실제적인 예시가 특징인 이 책은 SPE에 관한 비교할 수 없는 가장 최신 one-stop 소스로 어떠한 필드의 화학자에게도 잘 맞는다. 근본적인 원리, 응용, 새로운 기법들로 이루어진 각각의 섹션들로, 이책은 SPE 사용법과 실제 사용처에서부터 기기와 기법의 최근 진보에까지 최신 정보들을 제공하고 있다.
* 의학, 환경, 천연화합물화학에서의 SPE 응용에 관한 상세한 예들을 제공
* 화학자들이 흡착제(sorbent) 선택에 관해 정보가 되는 결정을 행할 수 있게 함
* 오토메이션, 새로운 시료 전처리 방법에 관해 귀중한 식견들로 최신 SPE 기법을 다루고 있음
* 더 깊이 있는 해석에 관한 제안, 인터넷 자원 및 제품 가이드등을 제공

• 저 자 : M. S. Mills, E. M. Thurman [John Wiley & Sons]
  
• ISBN : 047161422X
  
• Hardcover: 384 pages
  
• Dimensions (in inches): 0.98 x 9.38 x 6.35

 

Solid-Phase Extraction: Principles and Practice

 

Preface

Acknowledgments

Cumulative Listing of Volumes in Series

CHAPTER 1 OVERVIEW OF SOLID-PHASE EXTRACTION

1.1. What is Solid-Phase Extraction?

1.2. How to do Solid-Phase Extraction

1.3. Columns and Apparatus for Solid-Phase Extraction

1.4. Sorbents and Modes of Interaction

1.5. Applications of Solid-Phase Extraction

1.6. Automation of Solid-Phase Extraction

1.7. Manufacturers and Bibliographies

1.8. History and Future of Solid-Phase Extraction

Suggested Reading

References

 

CHAPTER 2 THEORY OF SORPTION AND ISOLATION

2.1. Introduction

2.2. Synthesis of Sorbents

2.2.1. The Silica Particle

2.2.2. Bonded Phases

2.2.3. Polymeric Sorbents

2.3. Mechanisms of Sorption

2.3.1. Reversed Phase

2.3.2. Normal Phase

2.3.3. Ion Exchange

2.3.4. Mixed Mode

2.4. Elution of Sorbents in Solid-Phase Extraction

2.4.1. Reversed Phase

2.4.2. Normal Phase

2.4.3. Ion Exchange and Mixed Mode

Suggested Reading

References

 

CHAPTER 3 METHODS DEVELOPMENT

3.1. Six-Step Approach to Methods Development

3.1.1. What is Solute Structure? The Clue to Effective Solid-Phase Extraction

3.1.2. Identify the Goal

3.1.3. Obtain Physical Constants

3.1.4. Choose the Mechanism of Solid-Phase Extraction

3.1.5. Elute the Solid-Phase Extraction Sorbent

3.1.6. Perform the Sorption Experiment and Determine Breakthrough

3.2. Executing the Solid-Phase Extraction Experiment in Five Steps

3.2.1. Step 1

3.2.2. Step 2

3.2.3. Step 3

3.2.4. Step 4

3.2.5. Step 5

3.3. Troubleshooting and Optimizing a Method

3.3.1. Problem 1: Incomplete Elution

3.3.2. Problem 2: Breakthrough of Analyte

3.3.3. Problem 3: Significant Breakthrough of Analyte

3.3.4. Problem 4: Interfering Substances

3.4. Critically Evaluate Previously Published Methods

3.5. Simple Summary of Methods Development Suggested Reading

References

 

CHAPTER 4 REVERSED-PHASE SOLID-PHASE EXTRACTION

4.1. Introduction

4.2. Structure of Reversed-Phase Sorbents

4.3. Reversed Phase as a Partitioning Mechanism

4.4. Chromatographic Plate Theory and Reversed-Phase Solid-Phase Extraction

4.4.1. Introduction

4.4.2. Theoretical Aspects of Plate Theory

4.5. Chromatographic Plate Theory: Its Application to Reversed-Phase Solid-Phase Extraction

4.5.1. Introduction

4.5.2. Determining and Predicting Breakthrough Volumes

4.5.3. Polarity and Breakthrough

4.5.4. Example Calculation of Breakthrough Volume using k'(w)

4.5.5. Practical Effects of Plate Number on Solid-Phase Extraction

4.6. Examples of Methods Development with Reversed-Phase Solid-Phase Extraction

4.6.1. Trace Enrichment of Pesticides from Groundwater

4.6.2. Extraction of Protein from Dilute Aqueous Solution

4.6.3. Extraction and Purification of Synthetic Oligonucleotides

4.6.4. Extraction of Indole-3-Acetic Acid

4.6.5. Extraction of Catecholamines from Urine

Suggested Reading

References

 

CHAPTER 5 NORMAL-PHASE SOLID-PHASE EXTRACTION

5.1. Introduction

5.2. Structure and Sorption of Normal-Phase Sorbents

5.3. Elution of Normal-Phase Sorbents

5.4. Examples of Methods Development with Normal-Phase Solid-Phase Extraction

5.4.1. Extraction of Aromatic Hydrocarbons from Crude Oil

5.4.2. Extraction of Polychlorinated Biphenyls from Transformer Oil

5.4.3. Extraction of Carotenes from Plant Tissue

5.4.4. Extraction of N-Nitrosoamine (N-Nitrosopyrrolidine) from Bacon

5.4.5. Extraction of Aflatoxins from Corn, Peanuts, and Peanut Butter

5.4.6. Extraction of Pyridonecarboxylic-Acid Antibacterials from Fish Tissue

5.4.7. Extraction of Vitamin D from Serum

5.4.8. Extraction of Antibiotics from Ointment

Suggested Reading

References

 

CHAPTER 6 ION-EXCHANGE SOLID-PHASE EXTRACTION

6.1. Introduction

6.2. Structure of Solid-Phase Extraction Ion-Exchanger Sorbents

6.2.1. Cartridges

6.2.2. Disks

6.3. Ion Exchange as a Chemical Reaction

6.4. Selectivity of Ion Exchange

6.5. Donnan Membrane Theory

6.6. Law of Chemical Equilibrium and Selectivity Coefficients

6.7. Kinetics of Ion Exchange

6.8. Methods Development: General Principles

6.8.1. Selecting Cation or Anion Exchange

6.8.2. Molecular Size and Weight

6.8.3. Interferences and Competing Ions

6.9. Methods Development Experiment

6.10. General Method for Ion-Exchange Solid-Phase Extraction

6.11. Examples Using Ion-Exchange Solid-Phase Extraction

6.11.1. Salt Conversions

6.11.2. Preparation of Deionized Water

6.11.3. Isolation of Metal Cations

6.11.4. Isolation of Triazine Herbicides from Soil

6.11.5. Purification of Organic Compounds

6.11.6. Hydroxyatrazine Metabolites from Water

6.11.7. Paraquat and Diaquat in Water

6.11.8. Food and Beverage

6.11.9. Food and Feeds

6.11.10. Pharmaceutical and Biological Applications

6.11.11. Extraction of Cimetidine from Urine

6.11.12. Dacthal Isolation and

Derivatization

Suggested Reading

References

 

CHAPTER 7 ENVIRONMENTAL ANALYSIS

7.1. Structure and Chemistry of Micropollutants

7.2. Generic Approach to Environmental Solid-Phase Extraction

7.3. Water Samples and Trace Enrichment

7.3.1. Introduction

7.3.2. Removal of Interferences

7.3.3. Generic Eluents

7.4. Environmental Protection Agency Methods

7.4.1. Cartridge Methods

7.4.2. Disk Methods

7.5. On-line Solid-Phase Extraction--High-Pressure Liquid Chromatography : Environmental Applications

7.6. Large-Volume Analysis by Solid-Phase Extraction

7.7. Soil Analysis and Solid-Phase Extraction

7.7.1. Solid-Phase Extraction Cleanup

7.7.2. Trace Enrichment

7.7.3. Normal-Phase Solid-Phase Extraction of Soil Extracts

7.8. Air Analysis and Solid-Phase Extraction

7.9. Oil and Grease Analysis

7.10. Examples of Environmental Solid-Phase Extraction

7.10.1. Organochlorine Pesticides in Water

7.10.2. Organochlorine Pesticides in Soil and Sediment

7.10.3. Polyaromatic Hydrocarbons in Water and Soil

7.10.4. Nonionic Herbicides in Water and Soil

7.10.5. Organophosphorus Pesticides in Water and Soil

7.10.6. Nonvolatile Organic Compounds

: Carbamates, Substituted Amides, and Phenylureas in Water and Soil

7.10.7. Herbicide Metabolites in Water and Soil

7.10.8. Phenols and Chlorinated Phenols in Water and Soil

7.10.9. Acid Herbicides (2,4-D, 2,4,5-T, Dicamba) and Sulfourea Herbicides in Water and Soil

7.10.10. Anionic Surfactants in Water and Soil

Suggested Reading

References

 

CHAPTER 8 DRUGS AND PHARMACEUTICALS

8.1. Introduction

8.2. Structure and Chemistry of Drugs

8.3. Sample Matrix

8.4. Mixed-Mode Sorbents

8.5. Application of Mixed Mode

8.6. Sorbents for Drug Analysis

8.7. NIDA Drugs of Abuse

8.7.1. Marijuana

8.7.2. Cocaine

8.7.3. Phencyclidine

8.7.4. Amphetamines

8.7.5. Opiates

8.8. General Drug Analysis and Methods

8.9. Veterinary Applications

8.10. Examples of Methods for Pharmaceutical and Biological Analysis

8.10.1. Cyclosporine in Blood

8.10.2. Vitamin D in Serum

8.10.3. Lipids from Serum and Tissue

8.10.4. Vitamin B(12) in Urine or Aqueous Solution

8.11. Automation and On-line Solid-Phase Extraction for Drug Analysis

8.12. Disk Technology and Drug Analysis

8.13. Innovations in Solid-Phase Extraction for Drug Analysis

Suggested Reading

References

 

CHAPTER 9 FOOD AND NATURAL PRODUCTS

9.1. Liquefying and Extraction of Food Prod

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