(단종/별도문의)SOLID PHASE MICROEXTRACTION: THEORY AND PRACTICE >

• 저 자 : Janusz Pawliszyn [Vch Pub]
  
• ISBN : 0471190349

Solid Phase Microextraction : Theory and Practice

1. SOLID PHASE MICROEXTRACTION IN PERSPECTIVE

1.1 Overview

1.2 Solvent-Free Sample Preparation Techniques

References

2. OPERATING PRINCIPLES AND CONSTRUCTION OF SPME DEVICES

2.1 Historical Perspective on the Early Work

2.2 Basic Principle of Solid Phase Microextraction

2.3 Extraction Modes

2.4 Coatings

2.5 Experimental Parameters that Affect Extraction Efficiency

2.6 Derivatization

2.7 Interfaces to Analytical Instrumentation

2.8 Commercial Devices

References

3. THEORY OF SOLID PHASE MICROEXTRACTION

3.1 Introduction

3.2 Thermodynamics

3.3 Kinetics

3.4 Experimental Verification

References

4. SPME METHOD DEVELOPMENT

4.1 Coating Selection

4.2 Derivatization Reagent Selection

4.3 Extraction Mode Selection

4.4 Agitation Technique Selection

4.5 Selection of a Manual vs Automated System

4.6 Selection of Separation and/or Detection Technique

4.7 Optimization of Desorption Conditions

4.8 Optimization of Sample Volume

4.9 Determination of Extraction Time Profile in Pure Matrix

4.10 Determination of Extraction Time

4.11 Calculation of the Distribution Constant

4.12 Optimization of Extraction Conditions

4.13 Determination of Linear Dynamic Range of the Method for a Pure Matrix at Optimum Extraction Conditions

4.14 Selection of the Calibration Method

4.15 Optimization of Extraction Conditions for Heterogeneous Samples

4.16 Verification of the Equilibration Time, Sensitivity, and Linear Dynamic Range for a Complex Sample Matrices

4.17 Method Precision

4.18 Method Detection Limits

4.19 Validation

4.20 Automation

References

5. APPLICATIONS

5.1 Gaseous Matrix

5.2 Liquid Matrix

5.3 Solid Matrix

5.4 Environmental

5.5 Food and Pharmaceutical

5.6 Clinical and Forensic

5.7 Future Analytical Applications

5.8 Physicochemical Applications

References

6. EXPERIMENTS

6.1 Determination of BTEX in Water

6.2 Determination of Pesticides in Water

6.3 Determination of Caffeine in Beverages

A. THEORETICAL ANALYZES

A.1 Estimation of the Distribution Constant for an Internally Cooled Fiber

A.2 Analysis of Diffusion in and Near the Fiber Coating, without or with "In-Fibre" Derivatization

A.3 One-Dimensional Analysis of Diffusion in a Headspace SPME System

References

B. LIST OF ARTICLES PUBLISHED ON SPME APPLICATIONS Glossary

Index 

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